Client-Run Instrument
Trainer: Kiran Subedi
Thermogravimetric Analyzing (TGA) is commonly employed in research and testing to determine characteristics of materials such as degradation temperatures, absorbed moisture content, the level of inorganic and organic components in a compound, decomposition points of explosives and the presence of solvent residues. It is also often used to estimate the corrosion kinetics in high temperature oxidation.
The Cahn TherMax 500 TGA system specializes in demanding applications where high temperatures, pressures, and aggressive atmospheres are required. Pressure can be used to enhance or speed up reactions. The weight changes of a sample is measured over a given temperature and pressure range under specific environmental conditions.
The furnace temperature follows a temperature profile sequence established by the user in a method in the Thermax software. The software periodically records weight and pressure measurements and stores them on the computer.
After the measurement cycle or “run” is completed, the data file can be processed in the Analysis mode of the software. Raw or processed data may be plotted on the monitor display or on a graphics plotter, printed in tabular form, or copied on a separate diskette for archiving
The three parts of the Thermax 500 are the:
- Mainframe - the instrument hardware which includes: pressure balance, furnace vessel, stand and elevator.
- Console - which: houses the instrument electronics, displays data and warnings and connects the Thermax with the computer.
- Pressure/Flow Controller - which: controls pressure in the instrument, controls flow for three (3) gases and indicates pressure in the instrument.
- The Cahn Thermax 500 instrument measurea weight changes on samples of up to 100 grams, from room temperature to 1100°C, with a maximum sensitivity of one microgram.
- The furnace follows a precise temperature profile of ramps and isotherms, established by the user, under constant computer control.
- Gas flow and pressure is controlled by a pressure/flow controller.
- Time, weight and temperature data are acquired at defined intervals and the data is stored on the computer's hard disk.
- Cahn's Thermax software allows you to edit and perform analytical functions on your run data. A permanent record of the raw data or the processed data can be made by printing in tabular form or copying to a diskette.
Product Specifications:
Balance
| Capacity | |
| Weighing | 100 grams |
| Volume | 30 cc |
| Weighing Range | |
| Maximum Weight | ±10 g |
| Sensitivity | 1µg |
| Temperature Drift | 10 µg/°C |
| Accuracy at ambient temperature | <0.02% |
| Repeatability | <0.001% |
Furnace
| Temperature Range | |
| at ambient pressure | Up to 1100°C |
| at 1000 psi | Up to 1000°C |
| Maxiumum Heating Rate | 25°C/min |
| Temperature Repeatability | ±3°C |
Pressure Level
| Maximum Pressure at 25°C | 1500 psi |
|---|---|
| Maximum Pressure at 1000°C | 1000psi |
| Internal Volume | 0.3 liters |
| Thermocouple | 1/8" Chromel-Alumel |
| Atmospheres | Static or dynamic gases including H2O, alcohols, aldehydes, ketones, alkanes, dilute acids, H2, CO2. |
| Sensitivity | 1µg |
| Temperature Drift | 10µg/°C |
| Accuracy at Ambient Temperature | <0.02% |
| Repeatability | <0.001% |
From The Cahn Thermax 500 Operator's Manual