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  2. General Experiments Handouts

General Experiments Handouts

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Body
  • Abbreviated Command and Parameter List
  • Apodization
  • Arrayed NMR Experiments at Constant Temperature
  • APT
  • 13C Sensitivity for Mass Limited Samples Nano Probe vs 3mm 13C{1H}
  • COSY
  • DEPT for the U500, VXR500, and U400
  • Deuterated NMR Solvents
  • Deuterium 2H-NMR in the SCS NMR Lab - UI500NB Only
  • External Referencing of Samples
  • HETCOR
  • Homodecoupling
  • 1H{31P} — Phosphorus Decoupled Proton NMR on the UI400 or U500
  • Locking
  • Manipulation of Multiple Spectra
  • 90 Degree Pulse Width Determination
  • NMR Chemical Shifts
  • NOE 1D Difference Experiment-cyclenoe NOE
  • NOESY1D-(DPFGSE NOE) Experiment for Measurement of Transient NOE’s
  • Optimizing 1D Array Acquisition Parameters
  • Performing the H-1 and F-19 NOE Experiment
  • Phase Sensitive 2D Data
  • Phosphorus 31 Standard QUAD Probe [1H/19F] - [15N-31P] Broadband Probe
  • Processing and Phasing Phase-Sensitive 2D Data (includes gHMQC, gHSQC)
  • Quick Instructions for No-D NMR or How to Take a Spectrum of Your Reaction Mixture
  • Quick pw90 (90 Degree Pulse Width) Determination
  • Quick T1 Determination
  • Sample Preparation, Positioning, and Insertion
  • Selective Decoupling: Homo-Decoupling of 1H-19F
  • Shimming
  • Shimming an NMR Magnet
  • Solvent Pre-Saturation - Suppression of the Solvent Peak
  • Solvent Pre-Saturation of Two Peaks - Double Solvent Suppression
  • T1 Measurement
  • T2 Determination
  • User Macros
  • UI500NB Advanced 1D and 2D NMR
  • Variable Temperature Control Using a Cold Bath
  • Variable Temperature Control Including Use of the FTS Unit
College of Liberal Arts & Sciences School of Chemical Sciences
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106 Noyes Lab, Box D-5, MC-712

505 S. Mathews Ave.

Urbana, IL 61801

217-333-5070

Email: scs-webmaster@illinois.edu

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NOTE: Do not send scientific samples to this address. Submission addresses can be found on the appropriate lab pages

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