College of Liberal Arts & Sciences School of Chemical Sciences
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Home Resources General Experiments Handouts

General Experiments Handouts

NMR Lab

Home ChemFOM Spectrometer Status Now Carver B500 Sample Queue B600 Sample Queue NMR Rates Instruments Instructional Handouts and Tools Mnova Software Basic Training Packet Schedules/Protocols DCM Use for NMR Directors' Presentations NMR Staff Publications Chemistry Resources Helium Shortage 55 NL Activities A151 CLSL Activities NMR Staff NMR Instrument Locations

Research

Research Cell Media Facility Electronic Services EPR Lab Glass Shop High-throughput Screening Facility Machine Shop Mass Spectrometry Lab Microanalysis Laboratory NMR Laboratory X-Ray Laboratory
  • Abbreviated Command and Parameter List
  • Apodization
  • Arrayed NMR Experiments at Constant Temperature
  • APT
  • 13C Sensitivity for Mass Limited Samples Nano Probe vs 3mm 13C{1H}
  • COSY
  • DEPT for the U500, VXR500, and U400
  • Deuterated NMR Solvents
  • Deuterium 2H-NMR in the SCS NMR Lab - UI500NB Only
  • External Referencing of Samples
  • HETCOR
  • Homodecoupling
  • 1H{31P} — Phosphorus Decoupled Proton NMR on the UI400 or U500
  • Locking
  • Manipulation of Multiple Spectra
  • 90 Degree Pulse Width Determination
  • NMR Chemical Shifts
  • NOE 1D Difference Experiment-cyclenoe NOE
  • NOESY1D-(DPFGSE NOE) Experiment for Measurement of Transient NOE’s
  • Optimizing 1D Array Acquisition Parameters
  • Performing the H-1 and F-19 NOE Experiment
  • Phase Sensitive 2D Data
  • Phosphorus 31 Standard QUAD Probe [1H/19F] - [15N-31P] Broadband Probe
  • Processing and Phasing Phase-Sensitive 2D Data (includes gHMQC, gHSQC)
  • Quick Instructions for No-D NMR or How to Take a Spectrum of Your Reaction Mixture
  • Quick pw90 (90 Degree Pulse Width) Determination
  • Quick T1 Determination
  • Sample Preparation, Positioning, and Insertion
  • Selective Decoupling: Homo-Decoupling of 1H-19F
  • Shimming
  • Shimming an NMR Magnet
  • Solvent Pre-Saturation - Suppression of the Solvent Peak
  • Solvent Pre-Saturation of Two Peaks - Double Solvent Suppression
  • T1 Measurement
  • T2 Determination
  • User Macros
  • UI500NB Advanced 1D and 2D NMR
  • Variable Temperature Control Using a Cold Bath
  • Variable Temperature Control Including Use of the FTS Unit
College of Liberal Arts & Sciences School of Chemical Sciences
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Urbana, IL 61801

217-333-5070

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